High pressure, high temperature, and low temperature parallel synthesis reactor

High pressure, high temperature, and low temperature parallel synthesis reactor

Detailed configuration specifications: Basic element [Schlenk * 12/30ML * 220 ℃ * Parallel magnetic force * Reflux * High pressure reaction below 6MPa * Online vacuum pumping below 0.1MPa * Each test tube can be individually controlled * Safety protection * Cleanable clean air chamber * Water gas source platform]+Function items [Intelligent heating magnetic stirrer IKA-RCT/Domestic magnetic stirrer]

Main technical parameters: (are the conventional indicators of this type of instrument product)

Advantageous technical indicators: (for indicators that are superior to similar imported products)

Basic Parameters:

1. Reaction site: position 12

2. Reaction vessel: 12 positions: 30 ML high-pressure test tube size: diameter 22mm * 156mm (single port high-pressure test tube)

3. Applicable volume: 5-30 ML

4. Scope of application: Magnetic stirring reaction, high temperature and high pressure reaction, reflux reaction, gas reaction, anhydrous and anaerobic reaction, airbag hydrogenation reaction below 6MPa, high vacuum reaction below -01MPa, can achieve immediate gas extraction.

5. Independent temperature zone: 1 heating and temperature control zone

6. Thermal conduction method: Solid state conduction module

7. Overnight experiment: Yes

8. Reflux efficiency: Reflux efficiency ≥ 90% (loss rate ≤ 15% when ethanol is heated and refluxed at 80 ℃ for 48 hours)

9. Condensation method 1: Water free air condensation (suitable for slight reflux of high boiling point solvents, B.P. ≥ 80 ℃)

10. Condensation method 2: External tap water cooling or external ethanol low-temperature circulating liquid (suitable for high-temperature reflux of low boiling point solvents, B.P. ≤ 80 ℃)

11. Can it be used for low-temperature reaction: The 12 position low-temperature circulating liquid pump can be used for low-temperature reaction within minus 20 ℃.

12. Connection method: Thread lock (new design experience, traditional thread connection and clip, high-pressure test tube uses thread connection to ensure a tight lock and prevent sticking)